methyl N-cyclopropylcarbamate

Base Information

Chemical Name:methyl N-cyclopropylcarbamate
CAS No.:220845-66-9
Molecular Formula:C₂₁H₂₅NO₄
Molecular Weight:355.434
Hs Code.:

methyl N-<cis-2,cis-3-bis(benzyloxymethyl)>cyclopropylcarbamate

Synonyms:methyl N-cyclopropylcarbamate

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Chemical Property of methyl N-cyclopropylcarbamate

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Technology Process of methyl N-cyclopropylcarbamate

There total 3 articles about methyl N-cyclopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 67-56-1
methanol

: 220842-46-6
cis-2,cis-3-bis(benzyloxymethyl)cyclopropanecarboxylic acid

: 220845-66-9
methyl N-cyclopropylcarbamate

Guidance literature:: With potassium hydroxide; [bis(acetoxy)iodo]benzene; at 5 - 20 ℃; for 1h;
DOI:10.1016/S0040-4020(98)01120-X

Reference yield:

: 172688-27-6
(1S,2R,3S)-2,3-Bis-benzyloxymethyl-cyclopropanecarbaldehyde

: 220845-66-9
methyl N-cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / Jones' reagent / acetone / 10 h / -5 °C

2: 1.) ClCO₂Et, Et₃N, 2.) NH₃ / 1.) THF, -5 deg C, 1 h, 2.) THF, 0 deg C, 1 h

3: 78 percent / KOH, PhI(OAc)2 / 1 h / 5 - 20 °C

With potassium hydroxide; jones' reagent; [bis(acetoxy)iodo]benzene; ammonia; chloroformic acid ethyl ester; triethylamine; In acetone;
DOI:10.1016/S0040-4020(98)01120-X

Reference yield:

: 220845-64-7
cis-2,cis-3-bis(benzyloxymethyl)cyclopropanecarboxylic acid

: 220845-66-9
methyl N-cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ClCO₂Et, Et₃N, 2.) NH₃ / 1.) THF, -5 deg C, 1 h, 2.) THF, 0 deg C, 1 h

2: 78 percent / KOH, PhI(OAc)2 / 1 h / 5 - 20 °C

With potassium hydroxide; [bis(acetoxy)iodo]benzene; ammonia; chloroformic acid ethyl ester; triethylamine;
DOI:10.1016/S0040-4020(98)01120-X