3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1⁽¹⁷⁾,13,15-triene

Base Information

• Chemical Name: 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1⁽¹⁷⁾,13,15-triene
• CAS No.: 102363-22-4
• Molecular Formula: C₃₃H₃₉N₅
• Molecular Weight: 505.706

Synonyms:3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1⁽¹⁷⁾,13,15-triene

Chemical Property of 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1⁽¹⁷⁾,13,15-triene

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Technology Process of 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1⁽¹⁷⁾,13,15-triene

There total 5 articles about 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1⁽¹⁷⁾,13,15-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-chloromethylpyridine hydrochloride (6959-47-3) + 3,11-dibenzyl-3,7,11,17-tetra-azabicyclo<11.3.1>heptadeca-1(17),13,15-triene (102363-20-2) → 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1(17),13,15-triene (102363-22-4)

Guidance literature:

With sodium hydroxide; In chloroform; at 50 ℃; for 72h;

DOI:10.1039/c39850001731

Reference yield: 78.0%

2-chloromethylpyridine (4377-33-7) + 3,11-dibenzyl-3,7,11,17-tetra-azabicyclo<11.3.1>heptadeca-1(17),13,15-triene (102363-20-2) → 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1(17),13,15-triene (102363-22-4)

Guidance literature:

With sodium hydroxide; In methanol; for 72h; Ambient temperature;

Reference yield:

bis(3-aminopropyl)amine (56-18-8) → 3,11-dibenzyl-7-(2'-pyridylmethyl)-3,7,11,17-tetra-azabicyclo(11.3.1)heptadeca-1(17),13,15-triene (102363-22-4)

Guidance literature:

Multi-step reaction with 3 steps

2: 53 percent / aq.NaOH / CHCl₃ / Ambient temperature

3: 80 percent / aq. NaOH / CHCl₃ / 72 h / 50 °C

With sodium hydroxide; In chloroform;

DOI:10.1039/c39850001731

upstream raw materials:

2-chloromethylpyridine

3,11-dibenzyl-3,7,11,17-tetra-azabicyclo<11.3.1>heptadeca-1(17),13,15-triene

2-chloromethylpyridine hydrochloride

bis(3-aminopropyl)amine

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