N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

Base Information

Chemical Name:N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine
CAS No.:862107-62-8
Molecular Formula:C₄₈H₅₁NO₃Si
Molecular Weight:718.023
Hs Code.:

Synonyms:N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

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Chemical Property of N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

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Technology Process of N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

There total 5 articles about N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butynyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

: 862107-62-8
N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethyl acetate; at 20 ℃; for 3h;
DOI:10.1021/ol050578j

Reference yield:

: 862107-60-6
C₂₆H₃₁NO₂Si

: 862107-62-8
N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Zn(OSO₃CF₃); Et₃N / CH₂Cl₂ / 20 °C

2: 97 percent / H₂ / Lindlar catalyst / ethyl acetate / 3 h / 20 °C

With hydrogen; zinc trifluoromethanesulfonate; triethylamine; Lindlar's catalyst; In dichloromethane; ethyl acetate;
DOI:10.1021/ol050578j

Reference yield:

: 82816-38-4
1-trityloxy-2-propyne

: 862107-62-8
N-[1-(tert-butyldiphenylsilanyloxymethyl)-4-trityloxy-2-butenyl]-N-(1R)-(1-phenylethyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Zn(OSO₃CF₃); Et₃N / CH₂Cl₂ / 20 °C

2: 97 percent / H₂ / Lindlar catalyst / ethyl acetate / 3 h / 20 °C

With hydrogen; zinc trifluoromethanesulfonate; triethylamine; Lindlar's catalyst; In dichloromethane; ethyl acetate;
DOI:10.1021/ol050578j