2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

Base Information

Chemical Name:2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole
CAS No.:1268726-33-5
Molecular Formula:C₁₅H₁₈F₃NO
Molecular Weight:285.309
Hs Code.:

Synonyms:2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

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Chemical Property of 2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

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Technology Process of 2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

There total 4 articles about 2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1236303-20-0
2-(2-methoxy-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro-oxazole

: 920-39-8
isopropylmagnesium bromide

: 1268726-33-5
2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 448-36-2
2-methoxy-4-(trifluoromethyl)-benzoic acid

: 1268726-33-5
2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide; thionyl chloride / toluene / 3 h / 80 °C

1.2: 16 h / 0 - 20 °C

2.1: thionyl chloride / dichloromethane / 16 h / 0 - 20 °C

3.1: tetrahydrofuran / 0 - 20 °C

With thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 886500-49-8
2-methoxy-4-trifluoromethyl-benzoyl chloride

: 1268726-33-5
2-(2-isopropyl-4-trifluoromethyl-phenyl)-4,4-dimethyl-4,5-dihydro oxazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

1.2: 10 - 20 °C

2.1: tetrahydrofuran / 0 - 20 °C

In tetrahydrofuran; dichloromethane;