4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

Base Information

Chemical Name:4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride
CAS No.:1620293-68-6
Molecular Formula:C₁₂H₁₂BrN₃O₂*ClH
Molecular Weight:346.611
Hs Code.:

Synonyms:4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

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Chemical Property of 4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

Chemical Property:

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Technology Process of 4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

There total 4 articles about 4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1620293-66-4
tert-butyl ((5-((2-bromo-4-cyanophenoxy)methyl)-4,5-dihydroisoxazol-3-yl)methyl)carbamate

: 1620293-68-6
4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 0 - 20 ℃; for 12h;

Reference yield:

: 2315-86-8
3-bromo-4-hydroxybenzonitrile

: 1620293-68-6
4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; potassium iodide / acetone / 2 h / Reflux

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 20 °C

2.2: 36 h / 20 °C

3.1: hydrogenchloride / 1,4-dioxane / 12 h / 0 - 20 °C

With hydrogenchloride; N-chloro-succinimide; potassium carbonate; potassium iodide; In 1,4-dioxane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 2973-78-6
3-bromo-4-hydroxybenzylaldehyde

: 1620293-68-6
4-((3-(aminomethyl)-4,5-dihydroisoxazol-5-yl)methoxy)-3-bromobenzonitrile hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride / dimethyl sulfoxide / 2 h / 90 °C

2.1: potassium carbonate; potassium iodide / acetone / 2 h / Reflux

3.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 20 °C

3.2: 36 h / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 12 h / 0 - 20 °C

With hydrogenchloride; N-chloro-succinimide; hydroxylamine hydrochloride; potassium carbonate; potassium iodide; In 1,4-dioxane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;