(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

Base Information

Chemical Name:(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine
CAS No.:1356599-98-8
Molecular Formula:C₁₆H₁₃BrF₃NO
Molecular Weight:372.185
Hs Code.:

Synonyms:(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

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Technology Process of (E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

There total 2 articles about (E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 643-65-2
3-methyl benzophenone

: 1356599-98-8
(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; sodium acetate; acetic acid / 3 h / 80 °C

2.1: sodium hydride / N,N-dimethyl-formamide; benzene / 0.5 h / 0 °C

2.2: 1 h / 0 - 20 °C

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 8 h / 75 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydroxylamine hydrochloride; sodium acetate; sodium hydride; acetic acid; In tetrachloromethane; N,N-dimethyl-formamide; benzene;

Reference yield:

: 27428-63-3
(3-methylphenyl)phenylmethanone oxime

: 1356599-98-8
(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; benzene / 0.5 h / 0 °C

1.2: 1 h / 0 - 20 °C

2.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 8 h / 75 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrachloromethane; N,N-dimethyl-formamide; benzene;

Reference yield: 10.7%

: 2393-17-1
3-(4-aminophenyl)propionic acid

: 1356599-98-8
(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine

: 1356598-65-6
3-{4-[(3-{(E,Z)-phenyl[(2,2,2-trifluoroethoxy)imino]methyl}benzyl)amino]phenyl}propanoic acid

Guidance literature:: 3-(4-aminophenyl)propionic acid; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

(E,Z)-1-[3-(bromomethyl)phenyl]-1-phenyl-N-(2,2,2-trifluoroethoxy)methanimine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;