(Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

Base Information

Chemical Name:(Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate
CAS No.:1620878-51-4
Molecular Formula:C₁₅H₁₃ClN₄S
Molecular Weight:316.814
Hs Code.:

Synonyms:(Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

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Chemical Property of (Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

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Technology Process of (Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

There total 5 articles about (Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620782-78-6
2-chloro-4-isothiocyanato-N-phenylaniline

: 19981-17-0,20611-81-8,123092-13-7,17292-62-5
sodium cyanamide

: 74-88-4
methyl iodide

: 1620878-51-4
(Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

Guidance literature:: sodium cyanamide; With sodium methylate; In methanol; at 20 ℃; for 0.25h; Inert atmosphere;

2-chloro-4-isothiocyanato-N-phenylaniline; In methanol; at 20 ℃; for 1h; Inert atmosphere;

methyl iodide; In methanol; at 20 ℃; Inert atmosphere;

Reference yield:

: 62-53-3
aniline

: 1620878-51-4
(Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 65 °C / Inert atmosphere; Cooling with ice

2.1: iron; ammonium chloride / water; methanol / 8 h / Inert atmosphere; Reflux

3.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

4.1: sodium methylate / methanol / 0.25 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

4.3: 20 °C / Inert atmosphere

With sodium methylate; iron; sodium hydride; ammonium chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 16611-23-7
2-chloro-4-nitro-N-phenylaniline

: 1620878-51-4
(Z)-methyl N-3-chloro-4-(phenylamino)phenyl-N'-cyanocarbamimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iron; ammonium chloride / water; methanol / 8 h / Inert atmosphere; Reflux

2.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

3.1: sodium methylate / methanol / 0.25 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

3.3: 20 °C / Inert atmosphere

With sodium methylate; iron; ammonium chloride; In methanol; dichloromethane; water;