tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

Base Information

Chemical Name:tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate
CAS No.:1345822-98-1
Molecular Formula:C₄H₄O₄*C₂₂H₂₆F₃NO₂
Molecular Weight:509.523
Hs Code.:

Synonyms:tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

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Chemical Property of tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

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Technology Process of tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

There total 3 articles about tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345822-93-6
tert-butyl 3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)-but-2-enoate

: 110-16-7,26099-09-2
maleic acid

: 1345822-98-1
tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

Guidance literature:: tert-butyl 3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)-but-2-enoate; With hydrogen; platinum on carbon; In isopropyl alcohol; at 35 ℃; under 2942.29 Torr;

maleic acid; In isopropyl alcohol; for 1h; Reflux;

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 1345822-98-1
tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / tert-butyl alcohol / 8 h / 30 - 82 °C

2.1: hydrogen / platinum on carbon / isopropyl alcohol / 35 °C / 2942.29 Torr

2.2: 1 h / Reflux

With hydrogen; acetic acid; platinum on carbon; In isopropyl alcohol; tert-butyl alcohol;

Reference yield:

: 764667-64-3
5-(1-hydroxy-2-(2,4,5-trifluorophenyl)ethylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1345822-98-1
tert-butyl (3R)-3-[[(1R)-1-phenylethyl]amino]-4-(2,4,5-trifluorophenyl)butanoate maleate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / tert-butyl alcohol / 8 h / 30 - 82 °C

2.1: hydrogen / platinum on carbon / isopropyl alcohol / 35 °C / 2942.29 Torr

2.2: 1 h / Reflux

With hydrogen; acetic acid; platinum on carbon; In isopropyl alcohol; tert-butyl alcohol;