Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

Base Information

Chemical Name:Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester
CAS No.:1053251-61-8
Molecular Formula:C₄₃H₅₁NO₁₀Si
Molecular Weight:769.964
Hs Code.:

Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

Synonyms:Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

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Chemical Property of Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

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Technology Process of Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

There total 3 articles about Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20160-60-5
2-(trimethylsilyl)-ethoxycarbonyl chloride

: 1053251-61-8
Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1) LHMDS / 1) THF, -78 deg C, 2) THF, -78 deg C

With lithium hexamethyldisilazane;
DOI:10.1021/jo980024c

Reference yield:

: 204579-03-3
1-amino-2,3,4,6-tetra-O-benzyl-1-deoxy-D-glucopyranose

: 1053251-61-8
Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1) LHMDS / 1) THF, -78 deg C, 2) THF, -78 deg C

With lithium hexamethyldisilazane;
DOI:10.1021/jo980024c

Reference yield:

: 5781-53-3
monomethyl oxalyl chloride

: 204579-04-4
((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid 2-trimethylsilanyl-ethyl ester

: 1053251-61-8
Oxo-[(2-trimethylsilanyl-ethoxycarbonyl)-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-amino]-acetic acid methyl ester

Guidance literature:: With lithium hexamethyldisilazane; Yield given. Multistep reaction; 1) THF, -78 deg C, 2) THF, -78 deg C;
DOI:10.1021/jo980024c