(E)-2,2'-diazidostilbene

Base Information

Chemical Name:(E)-2,2'-diazidostilbene
CAS No.:178265-14-0
Molecular Formula:C₁₄H₁₀N₆
Molecular Weight:262.274
Hs Code.:

Synonyms:(E)-2,2'-diazidostilbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2,2'-diazidostilbene

Chemical Property:

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Technology Process of (E)-2,2'-diazidostilbene

There total 4 articles about (E)-2,2'-diazidostilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 42467-40-3
2,2'-dinitrostilbene

: 178265-14-0
(E)-2,2'-diazidostilbene

Guidance literature:: With hydrogenchloride; sodium azide; sodium nitrite; In water; at 0 ℃;
DOI:10.1021/jo951789c

Reference yield:

: 6275-02-1
1,2-bis(o-nitrophenyl)ethylene

: 178265-14-0
(E)-2,2'-diazidostilbene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / PhSH, AINB / Heating

2: 94 percent / NaNO₂, HCl, NaN₃ / H₂O / 0 °C

With hydrogenchloride; sodium azide; thiophenol; sodium nitrite; In water;
DOI:10.1021/jo951789c

Reference yield:

: 23308-83-0
(2-nitrobenzyl)triphenylphosphonium bromide

: 178265-14-0
(E)-2,2'-diazidostilbene

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, dibenzo-18-crown-6 / CH₂Cl₂ / 16 h / Ambient temperature

2: 94 percent / NaNO₂, HCl, NaN₃ / H₂O / 0 °C

With hydrogenchloride; dibenzo-18-crown-6; sodium azide; potassium carbonate; sodium nitrite; In dichloromethane; water;
DOI:10.1021/jo951789c