methyl (E)-3-<(benzyloxy)amino>-2-propenoate

Base Information

Chemical Name:methyl (E)-3-<(benzyloxy)amino>-2-propenoate
CAS No.:81790-26-3
Molecular Formula:C₂₄H₂₃NO₄
Molecular Weight:389.451
Hs Code.:

methyl (E)-3-<(benzyloxy)amino>-2-<p-(benzyloxy)phenyl>propenoate

Synonyms:methyl (E)-3-<(benzyloxy)amino>-2-propenoate

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Chemical Property of methyl (E)-3-<(benzyloxy)amino>-2-propenoate

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Technology Process of methyl (E)-3-<(benzyloxy)amino>-2-propenoate

There total 5 articles about methyl (E)-3-<(benzyloxy)amino>-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 622-33-3
N-benzyloxyamine

: 81790-25-2
methyl (E)-3-(dimethylamino)-2-propenoate

: 81790-26-3
methyl (E)-3-<(benzyloxy)amino>-2-propenoate

Guidance literature:: With camphor-10-sulfonic acid; In benzene; for 12h; Heating;
DOI:10.1021/jo00136a005

Reference yield: 35.0%

: 81790-29-6
(E)-3-[Benzyloxy-(3-oxo-butyryl)-amino]-2-(4-benzyloxy-phenyl)-acrylic acid methyl ester

: 81790-26-3
methyl (E)-3-<(benzyloxy)amino>-2-propenoate

: 81790-30-9
3-acetyl-1-(benzyloxy)-4-hydroxy-5-<(p-benzyloxy)phenyl>-2(1H)-pyridinone

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 22 ℃; for 24h;
DOI:10.1021/jo00136a005

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 81790-26-3
methyl (E)-3-<(benzyloxy)amino>-2-propenoate

Guidance literature:: Multi-step reaction with 4 steps

1: BF₃*OEt₂ / 12 h / Ambient temperature

2: anhydrous potassium carbonate / butan-2-one / 24 h / Heating

3: 89 percent / N,N,N',N'-tetramethylethylenediamine / 12 h / 200 °C

4: 100 percent / camphorsulfonic acid (CSA) / benzene / 12 h / Heating

With N,N,N,N,-tetramethylethylenediamine; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; potassium carbonate; In butanone; benzene;
DOI:10.1021/jo00136a005