2-(ChloroMethyl)-5-Methylpyridine hydrochloride

Base Information

• Chemical Name: 2-(ChloroMethyl)-5-Methylpyridine hydrochloride
• CAS No.: 71670-70-7
• Molecular Formula: C7H9Cl2N
• Molecular Weight: 178.061
• Hs Code.: 2933399090
• Mol file: 71670-70-7.mol

Synonyms:Pyridine,2-(chloromethyl)-5-methyl-, hydrochloride (9CI);2-(Chloromethyl)-5-methylpyridine hydrochloride;

Chemical Property of 2-(ChloroMethyl)-5-Methylpyridine hydrochloride

Chemical Property:

• Boiling Point: 251.7 °C at 760 mmHg
• Flash Point: 106 °C
• PSA: 12.89000
• LogP: 2.93080
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

2-(chloromethyl)-5-methylpyridinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(ChloroMethyl)-5-Methylpyridine hydrochloride

There total 7 articles about 2-(ChloroMethyl)-5-Methylpyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.3%

2-hydroxymethyl-5-methylpyridine (22940-71-2) → 2-(chloromethyl)-5-methyl-pyridine monohydrochloride (71670-70-7)

Guidance literature:

With thionyl chloride; for 0.5h; Reflux;

Reference yield:

2-hydroxymethyl-5-methylpyridine (22940-71-2) + thionyl chloride (7719-09-7) → 2-(chloromethyl)-5-methyl-pyridine monohydrochloride (71670-70-7)

Guidance literature:

In chloroform; at 0 ℃;

Reference yield:

2-hydroxymethyl-5-methylpyridine (22940-71-2) + pyrographite (7440-44-0) → 2-(chloromethyl)-5-methyl-pyridine monohydrochloride (71670-70-7)

Guidance literature:

With thionyl chloride;

upstream raw materials:

2-hydroxymethyl-5-methylpyridine

thionyl chloride

pyrographite

2,5-dimethylpyridine N-oxide

Downstream raw materials:

2-<<(p-bromophenyl)thio>methyl>-5-methylpyridine

C₃₇H₄₁FN₄O₃S

3-{3-tert-butylsulfanyl-5-(5-methyl-pyridin-2-ylmethoxy)-1-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-1H-indol-2-yl}-2,2-dimethyl-propionic acid ethyl ester

C₃₆H₃₉N₃O₄

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