C₄₄H₄₈N₂O₆

Base Information

• Chemical Name: C₄₄H₄₈N₂O₆
• CAS No.: 1319741-87-1
• Molecular Formula: C₄₄H₄₈N₂O₆
• Molecular Weight: 700.875
• Mol file: 1319741-87-1.mol

Synonyms:C₄₄H₄₈N₂O₆

Chemical Property of C₄₄H₄₈N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₄₈N₂O₆

There total 5 articles about C₄₄H₄₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4,8-dibromo-2,6-bis(2-ethylhexyl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone (1248460-18-5) + 4-methoxyphenylacetylen (768-60-5) → C44H48N2O6 (1319741-87-1)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; diisopropylamine; triphenylphosphine; In toluene; at 80 ℃;

DOI:10.1021/ma2009063

Reference yield:

4,8-dibromobenzo[1,2-c;4,5-c']difuran-1,3,5,7-tetraone (24848-78-0) → C44H48N2O6 (1319741-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / Reflux

2: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diisopropylamine; triphenylphosphine / toluene / 80 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; acetic acid; diisopropylamine; triphenylphosphine; In toluene; 2: Sonogashira coupling;

DOI:10.1021/ma2009063

Reference yield:

1,2,4,5-tetramethylbenzene (95-93-2) → C44H48N2O6 (1319741-87-1)

Guidance literature:

Multi-step reaction with 5 steps

1.1: bromine / tetrachloromethane / 54 °C / Darkness

1.2: Irradiation; Reflux

2.1: sodium vanadate; nitric acid / Reflux

3.1: 205 °C

4.1: acetic acid / Reflux

5.1: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diisopropylamine; triphenylphosphine / toluene / 80 °C

With sodium vanadate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; bromine; nitric acid; acetic acid; diisopropylamine; triphenylphosphine; In tetrachloromethane; toluene; 5.1: Sonogashira coupling;

DOI:10.1021/ma2009063

upstream raw materials:

4,8-dibromo-2,6-bis(2-ethylhexyl)pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetraone

4-methoxyphenylacetylen

1,2,4,5-tetramethylbenzene

1,4-dibromo-2,3,5,6-tetrakis(bromomethyl)benzene