1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

Base Information

Chemical Name:1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine
CAS No.:1202008-80-7
Molecular Formula:C₃₀H₃₁ClN₂O₂
Molecular Weight:487.041
Hs Code.:

Synonyms:1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

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Chemical Property of 1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

Chemical Property:

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Technology Process of 1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

There total 9 articles about 1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 923022-55-3
1-benzyloxy-7-chloro-6-fluoro-isoquinoline

: 4-(1-amino-1-phenyl-ethyl)-cyclohexanol hydrochloride

: 1202008-80-7
1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

Guidance literature:: 4-(1-amino-1-phenyl-ethyl)-cyclohexanol hydrochloride; With sodium hydride; In ISOPROPYLAMIDE; mineral oil; for 1h; Inert atmosphere;

1-benzyloxy-7-chloro-6-fluoro-isoquinoline; In ISOPROPYLAMIDE; mineral oil; at 60 ℃;

Reference yield:

: 100-39-0
benzyl bromide

: 1202008-80-7
1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver carbonate / tetrahydrofuran / 20 - 70 °C

2.1: sodium hydride / ISOPROPYLAMIDE; mineral oil / 1 h / Inert atmosphere

2.2: 60 °C

With sodium hydride; silver carbonate; In tetrahydrofuran; ISOPROPYLAMIDE; mineral oil;

Reference yield:

: 923022-53-1
7-chloro-6-fluoro-2H-isoquinolin-1-one

: 1202008-80-7
1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-cyclohexyl]-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver carbonate / tetrahydrofuran / 20 - 70 °C

2.1: sodium hydride / ISOPROPYLAMIDE; mineral oil / 1 h / Inert atmosphere

2.2: 60 °C

With sodium hydride; silver carbonate; In tetrahydrofuran; ISOPROPYLAMIDE; mineral oil;