4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide

Base Information

• Chemical Name: 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide
• CAS No.: 468087-07-2
• Molecular Formula: C₁₈H₂₂N₄OS
• Molecular Weight: 342.465
• Mol file: 468087-07-2.mol

Synonyms:4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide

Chemical Property of 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide

There total 1 articles about 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-(Diethylamino)salicylaldehyde (17754-90-4) + 4-Phenyl-3-thiosemicarbazide (5351-69-9) → 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide (468087-07-2)

Guidance literature:

With acetic acid; In methanol; at 80 ℃; Solvent;

DOI:10.1016/j.bioorg.2020.104554

Reference yield: 90.91%

bis(acetylacetonato)dioxidomolybdenum(VI) + 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide (468087-07-2) → [MoO2(O(p-Et2N)C6H4CHNNC(S)NHC6H5)]n

Guidance literature:

In acetonitrile; Mo compd. suspended in MeCN, ligand added, warmed for 6 h; filtered, washed with MeCN, dried; elem. anal.;

DOI:10.1002/zaac.200400495

Reference yield: 86.9%

methanol (67-56-1) + bis(acetylacetonato)dioxidomolybdenum(VI) + 4-(4-diethylamino)-2-hydroxybenzylidene-N-phenylhydrazinecarbothioamide (468087-07-2) → [MoO2(O(p-Et2N)C6H3CHNNC(S)NHC6H5)(methanol)]

Guidance literature:

In methanol; Mo compd. suspended in dry MeOH, ligand added, warmed for 5 h; concd. in vac., left overnight., filtered, washed with cold MeOH, dried;elem. anal.;

DOI:10.1002/zaac.200400495

upstream raw materials:

4-(Diethylamino)salicylaldehyde

4-Phenyl-3-thiosemicarbazide