N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

Base Information

Chemical Name:N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid
CAS No.:85304-35-4
Molecular Formula:C₃₃H₃₀N₂O₅
Molecular Weight:534.612
Hs Code.:

Synonyms:N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

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Chemical Property of N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

Chemical Property:

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Technology Process of N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

There total 4 articles about N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85304-32-1
N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

: 85304-35-4
N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / acetic acid / 2 h

2: NaHCO₃ / CH₂Cl₂ / 21 h / Ambient temperature

3: CrO₃ / acetone; aq. H₂SO₄ / 1 h / Ambient temperature

With chromium(VI) oxide; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In dichloromethane; sulfuric acid; acetic acid; acetone;
DOI:10.1002/jps.2600720115

Reference yield:

: 85304-34-3
N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

: 85304-35-4
N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

Guidance literature:: With chromium(VI) oxide; In sulfuric acid; acetone; for 1h; Yield given; Ambient temperature;
DOI:10.1002/jps.2600720115

Reference yield:

: 98-88-4
benzoyl chloride

: 85304-35-4
N-(2S-2-benzamido-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / CH₂Cl₂ / 21 h / Ambient temperature

2: CrO₃ / acetone; aq. H₂SO₄ / 1 h / Ambient temperature

With chromium(VI) oxide; sodium hydrogencarbonate; In dichloromethane; sulfuric acid; acetone;
DOI:10.1002/jps.2600720115