N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

Base Information

Chemical Name:N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol
CAS No.:85304-32-1
Molecular Formula:C₃₄H₃₄N₂O₅
Molecular Weight:550.654
Hs Code.:

Synonyms:N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

Chemical Property:

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Technology Process of N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

There total 6 articles about N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)aminoethanol

: 85304-32-1
N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

Guidance literature:: With sodium hydrogencarbonate; In acetone; 0 deg C, 5 h; RT, 1.5 h; 4 deg C, 64 h;
DOI:10.1002/jps.2600720115

Reference yield:

: 6372-14-1
N-((benzyloxy)carbonyl)-L-phenylalaninol

: 85304-32-1
N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine

2: acetonitrile / 20 - 70 °C

3: sodium carbonate

With dmap; sodium carbonate; triethylamine; In acetonitrile;
DOI:10.1002/psc.1362

Reference yield:

: 109453-49-8
(C₈H₇O₂)(NHCHCOO)(CH₂C₆H₅)(CO₂C₂H₅)

: 85304-32-1
N-(2S-2-benzyloxycarbonylamino-3-phenylpropyl)-N-(9-fluorenylmethyloxy-carbonyl)aminoethanol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate

2: dmap; triethylamine

3: acetonitrile / 20 - 70 °C

4: sodium carbonate

With dmap; sodium tetrahydroborate; sodium carbonate; triethylamine; In acetonitrile;
DOI:10.1002/psc.1362