3-phenylhexanoic methyl ester

Base Information

• Chemical Name: 3-phenylhexanoic methyl ester
• CAS No.: 102882-04-2
• Molecular Formula: C₁₃H₁₈O₂
• Molecular Weight: 206.285
• Mol file: 102882-04-2.mol

Synonyms:3-phenylhexanoic methyl ester

Chemical Property of 3-phenylhexanoic methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-phenylhexanoic methyl ester

There total 12 articles about 3-phenylhexanoic methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl <1-phenyl-2-(E)-butenyl>acetate (99903-37-4,114968-90-0) → 3-phenylhexanoic methyl ester (102882-04-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In benzene; for 21h; under 98800.1 Torr;

DOI:10.1021/jo00355a025

Reference yield: 80.0%

methanol (67-56-1) + 3-phenylhexanoic acid (5703-52-6) → 3-phenylhexanoic methyl ester (102882-04-2)

Guidance literature:

With sulfuric acid; at 20 ℃;

DOI:10.1002/chem.200701232

Reference yield: 73.0%

bromobenzene (108-86-1,52753-63-6) + methyl 3-hydroxyhexanoate (21188-58-9) → 3-phenylhexanoic methyl ester (102882-04-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; triphenylphosphine; 4,4'-di-tert-butyl-2,2'-bipyridine; lithium bromide; nickel dibromide; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 14h; Glovebox; Electrolysis;

DOI:10.1021/jacs.0c13093

upstream raw materials:

methyl <1-phenyl-2-(E)-butenyl>acetate

ethyl (E)-1-phenylbut-1-en-3-ol

(2E)-1-phenylbut-2-en-1-ol

(E)-1-acetoxy-1-phenyl-2-butene

Downstream raw materials:

3-(4-chlorosulfonyl-phenyl)hexanoic methyl ester