10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate

Base Information

Chemical Name:10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate
CAS No.:1239018-76-8
Molecular Formula:C₂₅H₃₁FN₄O₇S
Molecular Weight:550.608
Hs Code.:

10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate

Synonyms:10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate

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Chemical Property of 10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate

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Technology Process of 10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate

There total 1 articles about 10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

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Reference yield:

: 1239018-75-7
tert-butyl (2-((4-fluorobenzyl)carbamoyl)-3-hydroxy-4-oxo-6,7,8,9-tetrahydro-7,10-ethanopyrimido[1,2-a]azepin-10(4H)-yl)carbamate

: 7143-01-3
Methanesulfonic anhydride

: 1239018-76-8
10-tert-butoxycarbonylamino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate

Guidance literature:: tert-butyl (2-((4-fluorobenzyl)carbamoyl)-3-hydroxy-4-oxo-6,7,8,9-tetrahydro-7,10-ethanopyrimido[1,2-a]azepin-10(4H)-yl)carbamate; Methanesulfonic anhydride; With triethylamine; In acetonitrile; at 0 - 15 ℃; for 0.5h;

With water; In acetonitrile; at 0 ℃; for 2h;