1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

Base Information

Chemical Name:1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide
CAS No.:1034137-22-8
Molecular Formula:Br*C₂₇H₃₉N₂
Molecular Weight:471.524
Hs Code.:

Synonyms:1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

Suppliers and Price of 1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

Chemical Property:

Purity/Quality:: HPLC≥98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

There total 2 articles about 1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 106-93-4
ethylene dibromide

: 1176938-29-6,581776-24-1
N,N'-di(2,6-diisopropylphenyl)formamidine

: 1034137-22-8
1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1039/d1nj00514f

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1034137-22-8
1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 4 h / Reflux

2: potassium carbonate / acetonitrile / Reflux

With potassium carbonate; acetic acid; In acetonitrile;
DOI:10.1039/d0ob00036a

Reference yield: 90.0%

: 1034137-22-8
1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide

: palladium dichloride

: [(SIPr)PdCl2]

Guidance literature:: 1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

palladium dichloride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1039/d1nj00514f