(S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

Base Information

Chemical Name:(S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane
CAS No.:713143-73-8
Molecular Formula:C₂₁H₃₆O₃Si
Molecular Weight:364.601
Hs Code.:

Synonyms:(S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

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Chemical Property of (S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

Chemical Property:

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Technology Process of (S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

There total 2 articles about (S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 713143-72-7
(S)-1-(4-methoxy-benzyloxy)-5-methyl-hex-5-en-3-ol

: 994-30-9
triethylsilyl chloride

: 713143-73-8
(S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1002/anie.200453663

Reference yield:

: 195257-60-4
(2S)-2-[2-(p-methoxybenzyloxy)ethyl]oxirane

: 713143-73-8
(S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg; 1,2-dibromoethane / tetrahydrofuran / 0.25 h / Heating

1.2: 86 percent / CuI / tetrahydrofuran / 0.5 h / -60 °C

2.1: 97 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / 20 °C

With 1H-imidazole; dmap; magnesium; ethylene dibromide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.200453663

Reference yield: 95.0%

: 713143-73-8
(S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane

: 713143-74-9
(R)-6-(4-Methoxy-benzyloxy)-2-methyl-4-triethylsilanyloxy-hexan-1-ol

Guidance literature:: (S)-{1-[2-(4-methoxy-benzyloxy)-ethyl]-3-methyl-but-3-enyloxy}-triethylsilane; With borane-THF; In tetrahydrofuran; at 0 ℃; for 2h;

With sodium hydroxide; dihydrogen peroxide; In water; at 0 ℃; for 2h;
DOI:10.1002/anie.200453663