tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

Base Information

Chemical Name:tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate
CAS No.:223511-04-4
Molecular Formula:C₂₀H₃₆O₄Si₂
Molecular Weight:396.674
Hs Code.:

Synonyms:tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

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Technology Process of tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

There total 1 articles about tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2237-36-7
4-methoxysalicylic acid

: 18162-48-6
tert-butyldimethylsilyl chloride

: 223511-04-4
tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

Guidance literature:: With dmap; triethylamine; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2020.131437

Reference yield: 98.0%

: 109-89-7
diethylamine

: 223511-04-4
tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

: 460348-03-2
2-((tert-butyldimethylsilyl)oxy)-N,N-diethyl-4-methoxybenzamide

Guidance literature:: diethylamine; With trimethylaluminum; In toluene; at -6 - 20 ℃; for 0.75h;

tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate; In toluene; Heating;
DOI:10.1016/S0040-4039(02)00870-5

Reference yield:

: 223511-04-4
tert-butyldimethylsilyl 2-((tert-butyldimethylsilyl)oxy)-4-methoxybenzoate

: 2-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-benzoyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; 0 deg C -> r.t., 18 h;
DOI:10.1016/S0040-4039(99)00279-8