C₂₃H₂₂N₄O₃

Base Information

Chemical Name:C₂₃H₂₂N₄O₃
CAS No.:1246349-96-1
Molecular Formula:C₂₃H₂₂N₄O₃
Molecular Weight:402.453
Hs Code.:

C<sub>23</sub>H<sub>22</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₂N₄O₃

Suppliers and Price of C₂₃H₂₂N₄O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₂₂N₄O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₂₂N₄O₃

There total 6 articles about C₂₃H₂₂N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246349-90-5
4-chloro-1-(4-methoxy-benzyl)-3-methyl-1H-pyrazolo[4,3-c]pyridine

: C₁₅H₁₆ClN₃O

: 619-45-4
4-methoxycarbonyl aniline

: C₂₂H₂₀N₄O₃

: 1246349-96-1
C₂₃H₂₂N₄O₃

Guidance literature:: With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In 1,4-dioxane; at 90 ℃; for 18h; Inert atmosphere;

Reference yield:

: 26452-80-2
2,4-dichloropyridine

: 1246349-96-1
C₂₃H₂₂N₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2.5 h / -78 °C

1.2: 1.5 h / -78 °C

2.1: tetrahydrofuran / -78 - 20 °C

3.1: 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / Molecular sieves 4?

3.2: 2 h / 20 °C

4.1: hydrazine hydrate / 20 °C

5.1: potassium hydroxide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

6.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / 1,4-dioxane / 18 h / 90 °C / Inert atmosphere

With n-butyllithium; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; hydrazine hydrate; 4-methylmorpholine N-oxide; diisopropylamine; potassium hydroxide; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1246349-88-1
1-(2,4-dichloropyridin-3-yl)ethan-1-ol

: 1246349-96-1
C₂₃H₂₂N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / Molecular sieves 4?

1.2: 2 h / 20 °C

2.1: hydrazine hydrate / 20 °C

3.1: potassium hydroxide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / 1,4-dioxane / 18 h / 90 °C / Inert atmosphere

With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; hydrazine hydrate; 4-methylmorpholine N-oxide; potassium hydroxide; palladium diacetate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;