3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

Base Information

Chemical Name:3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene
CAS No.:1366650-58-9
Molecular Formula:C₂₂H₂₆ClO₂P
Molecular Weight:388.874
Hs Code.:

Synonyms:3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

Chemical Property:

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Technology Process of 3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

There total 5 articles about 3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 84441-27-0
C₁₀H₁₆Cl₃O₂P

: 100-58-3
phenylmagnesium bromide

: 1366650-58-9
3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

Guidance literature:: In diethyl ether; at -10 ℃; for 4h; Reflux;
DOI:10.1016/j.tetlet.2012.02.042

Reference yield:

: 75-97-8
3,3-dimethyl-butan-2-one

: 1366650-58-9
3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

Guidance literature:: Multi-step reaction with 5 steps

1: potassium tert-butylate

2: phosphorus trichloride / dichloromethane

3: chlorine / tetrachloromethane

4: Heating

5: diethyl ether / 4 h / -10 °C / Reflux

With potassium tert-butylate; chlorine; phosphorus trichloride; In tetrachloromethane; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2012.02.042

Reference yield:

: 14846-86-7
2-tert-butyl-4-(methoxymethyl)-3-butyn-2-ol

: 1366650-58-9
3-tert-butyl-2-chloro-1-methoxymethyl-1-diphenylphosphoryl-1,3-butadiene

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus trichloride / dichloromethane

2: chlorine / tetrachloromethane

3: Heating

4: diethyl ether / 4 h / -10 °C / Reflux

With chlorine; phosphorus trichloride; In tetrachloromethane; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2012.02.042