(Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

Base Information

Chemical Name:(Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate
CAS No.:1108179-33-4
Molecular Formula:C₂₁H₃₁O₈P
Molecular Weight:442.446
Hs Code.:

Synonyms:(Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

Suppliers and Price of (Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

There total 1 articles about (Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 814-49-3
diethyl chlorophosphate

: 108182-71-4
(Z)-3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hept-5-eno-1,4-furanose

: 1108179-33-4
(Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 ℃;
DOI:10.1039/b813978d

Reference yield:

: 1108179-33-4
(Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate

: 63959-88-6
tert-butyl N-(trifluoroacetyl)glycinate

: 1108179-41-4
5-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester

: 5-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-(2S)-(trifluoroacetyl)amino-4-(E)-pentenoic acid tert-butyl ester

: 1108179-42-5
5-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-(2R)-(trifluoroacetyl)amino-4-(E)-pentenoic acid tert-butyl ester

Guidance literature:: tert-butyl N-(trifluoroacetyl)glycinate; With zinc(II) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.333333h;

(Z)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl diethyl phosphate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; at -78 - 20 ℃; optical yield given as %de;
DOI:10.1039/b813978d