methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate

Base Information

• Chemical Name: methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate
• CAS No.: 790225-79-5
• Molecular Formula: C₃₀H₃₀F₃NO₇S
• Molecular Weight: 605.632

Synonyms:methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate

Chemical Property of methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate

Chemical Property:

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MSDS Files:

Useful:

Technology Process of methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate

There total 1 articles about methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) + methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-4-hydroxy-2-(phenylmethyl)-2,3-dihydro-1H-indole-2-carboxylate (790225-78-4) → methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate (790225-79-5)

Guidance literature:

With triethylamine; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 2.5h;

Reference yield:

methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate (790225-79-5) + phenylboronic acid (98-80-6) → methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-4-phenyl-2-(phenylmethyl)-2,3-dihydro-1H-indole-2-carboxylate (790225-88-6)

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 80 ℃; for 16h;

Reference yield:

methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-{[(trifluoromethyl)sulfonyl]oxy}-2,3-dihydro-1H-indole-2-carboxylate (790225-79-5) + thiazol-2-ylzinc(II) bromide (173382-28-0) → methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-(1,3-thiazol-2-yl)-2,3-dihydro-1H-indole-2-carboxylate (790225-90-0)

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 80 ℃; for 16h;

upstream raw materials:

N,N-phenylbistrifluoromethane-sulfonimide

methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-4-hydroxy-2-(phenylmethyl)-2,3-dihydro-1H-indole-2-carboxylate

Downstream raw materials:

2-methyl-4-(phenylmethyl)-1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-2,3-dihydro-1H-indole-2,4-dicarboxylate

methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-4-phenyl-2-(phenylmethyl)-2,3-dihydro-1H-indole-2-carboxylate

methyl 1-{[4-(1,1-dimethylethyl)-3-(methyloxy)phenyl]carbonyl}-2-(phenylmethyl)-4-(1,3-thiazol-2-yl)-2,3-dihydro-1H-indole-2-carboxylate

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