8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Base Information

Chemical Name:8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
CAS No.:36080-66-7
Molecular Formula:C₃₄H₃₈N₂O₄
Molecular Weight:538.687
Hs Code.:

8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo<b,k>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Synonyms:8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Chemical Property of 8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Technology Process of 8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

There total 6 articles about 8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

: 340963-59-9
1,2-bis[2-(N-benzylamino)ethoxy]benzene dihydrochloride

: 36080-66-7
8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With sodium perchlorate; sodium carbonate; In tetrahydrofuran; acetonitrile; at 80 ℃; for 36h;
DOI:10.1002/jhet.5570380142

Reference yield: 34.0%

: 55-51-6
N,N-bis(2-chloro-ethyl)-benzenemethanamine

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 36080-66-7
8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With sodium hydroxide; In butan-1-ol; at 110 ℃; for 18.75h;

Reference yield:

: 10234-40-9
2,2'-(1,2-phenylenedioxy)diethanol

: 36080-66-7
8,19-dibenzyl-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / 4 h / -10 °C

2: 72 percent / Na₂CO₃; NaClO₄*H₂O / tetrahydrofuran; acetonitrile / 36 h / 80 °C

With pyridine; sodium perchlorate; sodium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1002/jhet.5570380142