N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide

Base Information

• Chemical Name: N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide
• CAS No.: 337519-65-0
• Molecular Formula: C₂₈H₃₅N₃O₅S
• Molecular Weight: 525.669

Synonyms:N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide

Chemical Property of N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide

Chemical Property:

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Technology Process of N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide

There total 1 articles about N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-{4-[(1-t-butoxycarbonylpiperidin)-4-yloxy]phenyl}ethanesulfonamide (337519-64-9) + [3-(3-cyanophenyl)-2-(E)-propenyl]ethyl carbonate + ethyl acetate (141-78-6) → N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide (337519-65-0)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield: 44.0%

N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide (337519-65-0) + ammonium chloride + acetonitrile (75-05-8,26809-02-9) → N-[(E)-3-(3-amidinophenyl)-2-propenyl]-N-[4-(piperidin-4-yloxy)phenyl]ethanesulfonamide dihydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; ammonium hydroxide; ethanol; dichloromethane; water;

Reference yield:

N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]ethanesulfonamide (337519-65-0) + ethanol (64-17-5) → C25H33N3O4S

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 9h; Cooling with ice;

DOI:10.1248/cpb.56.758

upstream raw materials:

N-{4-[(1-t-butoxycarbonylpiperidin)-4-yloxy]phenyl}ethanesulfonamide

ethyl acetate

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