Dichlorocarbamic acid;fluoride

Base Information

• Chemical Name: Dichlorocarbamic acid;fluoride
• CAS No.: 32751-02-3
• Molecular Formula: CCl₂FNO
• Molecular Weight: 131.922
• DSSTox Substance ID: DTXSID90701892
• Mol file: 32751-02-3.mol

Synonyms:dichlorocarbamic acid;fluoride;DTXSID90701892

Chemical Property of Dichlorocarbamic acid;fluoride

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 147.9368368
• Heavy Atom Count: 7
• Complexity: 62.6

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C(=O)(N(Cl)Cl)O.[F-]

Technology Process of Dichlorocarbamic acid;fluoride

There total 3 articles about Dichlorocarbamic acid;fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

fluoroformyliminosulfur difluoride (3855-41-2) + chlorine monofluoride (7790-89-8) → N,N-dichloro-1-fluoroformamide (32751-02-3)

Guidance literature:

ratio of FC(O)NSF2:ClF = 1:2; at -78°C for 4 h;

DOI:10.1016/S0022-1139(00)83224-8

Reference yield: 40.0%

chlorine isocyanate (13858-09-8) + chlorine monofluoride (7790-89-8) → N,N-dichloro-1-fluoroformamide (32751-02-3)

Guidance literature:

With potassium fluoride; at -78°C for 0.5 h then 25°C for 1 h;

DOI:10.1021/ic50130a029

Reference yield:

→ N,N-dichloro-1-fluoroformamide (32751-02-3)

Guidance literature:

FC(O)NSF2, ClF;

DOI:10.1016/S0022-1139(00)83224-8

upstream raw materials:

chlorine isocyanate

chlorine monofluoride

fluoroformyliminosulfur difluoride

Downstream raw materials:

Carbonyl fluoride

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