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Technology Process of (Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2

(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2

Base Information
  • Chemical Name:(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2
  • CAS No.:102782-01-4
  • Molecular Formula:CH2Cl2*C65H54Cl3N2OP4Re2*F6P
  • Molecular Weight:1711.72
  • Hs Code.:
(Re<sub>2</sub>Cl<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2(CO)(NCC<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>*CH<sub>2</sub>Cl<sub>2</sub>=(Re<sub>2</sub>Cl<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2(CO)(NCC<sub>6</sub>H<sub>5</sub>)2)PF<sub>6</sub>*CH<sub>2</sub>Cl<sub>2</sub>

Synonyms:(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2

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Chemical Property of (Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2
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Technology Process of (Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2

There total 1 articles about (Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

thallium(I) hexafluorophosphate
60969-19-9

thallium(I) hexafluorophosphate

Re2(μ-Cl)(μ-dppm)2Cl3(CO)
96306-83-1,96306-79-5

Re2(μ-Cl)(μ-dppm)2Cl3(CO)

benzonitrile
100-47-0

benzonitrile

(Re<sub>2</sub>Cl<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2(CO)(NCC<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>*CH<sub>2</sub>Cl<sub>2</sub>=(Re<sub>2</sub>Cl<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2(CO)(NCC<sub>6</sub>H<sub>5</sub>)2)PF<sub>6</sub>*CH<sub>2</sub>Cl<sub>2</sub>
102782-01-4

(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)(1+)*PF6(1-)*CH2Cl2=(Re2Cl3((C6H5)2PCH2P(C6H5)2)2(CO)(NCC6H5)2)PF6*CH2Cl2

Guidance literature:
With dichloromethane; In dichloromethane; acetone; byproducts: TlCl; mixt. Re2Cl4(dppm)2(CO) and TlPF6 in acetone and benzonitrile allowed to react for 10 h at room temp., soln. filtered, filtrate reduced in volume under stream of N2, excess Et2O added, solid filtered off and redissolved in CH2Cl2; filtrate treated with Et2O; elem. anal.;
DOI:10.1021/ja00276a023
upstream raw materials:

thallium(I) hexafluorophosphate

Re2(μ-Cl)(μ-dppm)2Cl3(CO)

benzonitrile

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