methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

Base Information

Chemical Name:methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside
CAS No.:197657-33-3
Molecular Formula:C₄₁H₄₂O₁₂
Molecular Weight:726.777
Hs Code.:

Synonyms:methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

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Chemical Property of methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

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Technology Process of methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

There total 6 articles about methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73-34-7,87-96-7,488-79-9,551-63-3,609-01-8,643-17-4,643-18-5,4164-09-4,6014-42-2,6155-36-8,6189-71-5,6696-41-9,6736-43-2,13224-93-6,22611-09-2,28161-49-1,28161-50-4,28161-52-6,45864-36-6,63814-64-2,71116-59-1,71116-61-5,72598-05-1,87936-88-7,87936-89-8,97466-79-0,116908-82-8,120442-60-6,123484-22-0,133576-32-6
D-Fucose

: 197657-33-3
methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Py / CH₂Cl₂ / 20 °C

2: HBr / CHCl₃

3: 1.) Hg(CN)2, HgBr₂, molecular sieves 4 Angstroem / 1.) CH₃CN, 20 deg C, 45 min, 2.) CH₃CN, 1 h

With pyridine; 4 A molecular sieve; hydrogen bromide; mercury(II) cyanide; mercury dibromide; In dichloromethane; chloroform;

Reference yield:

: 98-88-4
benzoyl chloride

: 197657-33-3
methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Py / CH₂Cl₂ / 20 °C

2: HBr / CHCl₃

3: 1.) Hg(CN)2, HgBr₂, molecular sieves 4 Angstroem / 1.) CH₃CN, 20 deg C, 45 min, 2.) CH₃CN, 1 h

With pyridine; 4 A molecular sieve; hydrogen bromide; mercury(II) cyanide; mercury dibromide; In dichloromethane; chloroform;

Reference yield:

: 197657-32-2
(2R,3R,4S,5S,6R)-6-methyltetrahydro-2H-pyran-2,3,4,5-tetrayl tetrabenzoate

: 197657-33-3
methyl 2-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-fucopyranosyl)-β-D-quinovopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: HBr / CHCl₃

2: 1.) Hg(CN)2, HgBr₂, molecular sieves 4 Angstroem / 1.) CH₃CN, 20 deg C, 45 min, 2.) CH₃CN, 1 h

With 4 A molecular sieve; hydrogen bromide; mercury(II) cyanide; mercury dibromide; In chloroform;