methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

Base Information

Chemical Name:methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate
CAS No.:287952-12-9
Molecular Formula:C₁₉H₂₄F₃NO₆S
Molecular Weight:451.464
Hs Code.:

Synonyms:methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

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Technology Process of methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

There total 4 articles about methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5414-19-7
1,1'-oxybis(2-bromo-ethane)

: 287952-11-8
methyl [[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]acetate

: 287952-12-9
methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

Guidance literature:: With potassium carbonate; In N-methyl-acetamide; ethyl acetate;

Reference yield:

: 287952-10-7
1-(methylsulfonyl)-4-[4-(trifluoromethyl)phenoxy]piperidine

: 287952-12-9
methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; lithium hexamethyldisilazane / tetrahydrofuran

2: potassium carbonate / N-methyl-acetamide; ethyl acetate

With ammonium chloride; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; N-methyl-acetamide; ethyl acetate;

Reference yield:

: 28033-37-6
4-[4-(trifluoromethyl)-phenoxy]piperidine

: 287952-12-9
methyl tetrahydro-4-[[4-[4-(trifluoromethyl)phenoxy]-1-piperidinyl]sulfonyl]-2H-pyran-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether; dichloromethane; ethyl acetate

2: ammonium chloride; lithium hexamethyldisilazane / tetrahydrofuran

3: potassium carbonate / N-methyl-acetamide; ethyl acetate

With ammonium chloride; potassium carbonate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; N-methyl-acetamide; diethyl ether; dichloromethane; ethyl acetate;