1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin

Base Information

Chemical Name:1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin
CAS No.:88453-15-0
Molecular Formula:C₁₆H₁₆O
Molecular Weight:228.271
Hs Code.:

Synonyms:1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin

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Technology Process of 1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin

There total 2 articles about 1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88441-18-3
3-phenyl-1-tetralone-2,2-d₂

: 88453-15-0
1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin

Guidance literature:: With lithium aluminium deuteride; water-d2; Yield given. Multistep reaction; 1) ether, reflux, 3 h; 2) ether;
DOI:10.1021/ja00318a031

Reference yield:

: 14944-26-4
3-phenyl-1-tetralone

: 88453-15-0
1,2,2-trideuterio-1-deuteroxy-3-phenyltetralin

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / D₂O, K₂CO₃ / 16 h / Heating

2: 1) LiAlD₄; 2) D₂O / 1) ether, reflux, 3 h; 2) ether

With lithium aluminium deuteride; water-d2; potassium carbonate;
DOI:10.1021/ja00318a031