meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

Base Information

Chemical Name:meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene
CAS No.:217025-90-6
Molecular Formula:C₂₄H₃₄O₅
Molecular Weight:402.531
Hs Code.:

Synonyms:meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

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Technology Process of meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

There total 3 articles about meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3282-30-2
pivaloyl chloride

: 217025-86-0
meso-(1R,4S,6s)-6-(benzyloxy)cyclohept-2-ene-1,4-diol

: 217025-90-6
meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

Guidance literature:: With pyridine; dmap; for 16h; Heating;
DOI:10.1021/jo981102z

Reference yield:

: 115522-58-2
6-(benzyloxy)-1,3-cycloheptadiene

: 217025-90-6
meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / benzoquinone; MnO₂ / palladium(II) acetate / acetic acid / 20 °C

2: 93 percent / aq. KOH / methanol / 0.5 h / 0 °C

3: 99 percent / DMAP; pyridine / 16 h / Heating

With pyridine; dmap; manganese(IV) oxide; potassium hydroxide; p-benzoquinone; palladium diacetate; In methanol; acetic acid; 1: Acetoxylation / 2: Hydrolysis / 3: Esterification;
DOI:10.1021/jo981102z

Reference yield:

: 217025-84-8
meso-(3R,5s,7S)-5-(benzyloxy)-3,7-diacetoxycyclohept-1-ene

: 217025-90-6
meso-(3R,5s,7S)-5-(benzyloxy)-3,7-bis((2,2-dimethylpropionyl)oxy)cyclohept-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / aq. KOH / methanol / 0.5 h / 0 °C

2: 99 percent / DMAP; pyridine / 16 h / Heating

With pyridine; dmap; potassium hydroxide; In methanol; 1: Hydrolysis / 2: Esterification;
DOI:10.1021/jo981102z