2-iodo-5-trimethylsilylethynylbenzoic acid

Base Information

Chemical Name:2-iodo-5-trimethylsilylethynylbenzoic acid
CAS No.:251564-40-6
Molecular Formula:C₁₂H₁₃IO₂Si
Molecular Weight:344.224
Hs Code.:

Synonyms:2-iodo-5-trimethylsilylethynylbenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-iodo-5-trimethylsilylethynylbenzoic acid

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Technology Process of 2-iodo-5-trimethylsilylethynylbenzoic acid

There total 2 articles about 2-iodo-5-trimethylsilylethynylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 14192-12-2
2,5-diiodobenzoic acid

: 1066-54-2
trimethylsilylacetylene

: 251564-40-6
2-iodo-5-trimethylsilylethynylbenzoic acid

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4039(99)01697-4

Reference yield: 14.0%

: 14192-12-2
2,5-diiodobenzoic acid

: 1066-54-2
trimethylsilylacetylene

: 251564-40-6
2-iodo-5-trimethylsilylethynylbenzoic acid

: 3-methylene-6-trimethylsilanylethynyl-3H-isobenzofuran-1-one

: 6-trimethylsilanylethynyl-3-(3-trimethylsilanyl-prop-2-ynylidene)-3H-isobenzofuran-1-one

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(99)01697-4