isophthalic acid bis(2,2-dimethylhydrazide)

Base Information

• Chemical Name: isophthalic acid bis(2,2-dimethylhydrazide)
• CAS No.: 16538-38-8
• Molecular Formula: C₁₂H₁₈N₄O₂
• Molecular Weight: 250.301

Synonyms:isophthalic acid bis(2,2-dimethylhydrazide)

Chemical Property of isophthalic acid bis(2,2-dimethylhydrazide)

Chemical Property:

Purity/Quality:

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Technology Process of isophthalic acid bis(2,2-dimethylhydrazide)

There total 2 articles about isophthalic acid bis(2,2-dimethylhydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N,N-Dimethylhydrazine (57-14-7) + benzene-1,3-dicarbonyl dichloride (99-63-8) → isophthalic acid bis(2,2-dimethylhydrazide) (16538-38-8)

Guidance literature:

With triethylamine; In dichloromethane; 1.) 0 deg C, 2 h, 2.) 25 deg C, 18 h;

DOI:10.1002/jps.2600750419

Reference yield:

→ isophthalic acid bis(2,2-dimethylhydrazide) (16538-38-8)

Guidance literature:

/BRN= 889138/, H2NN(CH3)2;

Reference yield: 94.0%

isophthalic acid bis(2,2-dimethylhydrazide) (16538-38-8) + methyl iodide (74-88-4) → 2,2'-isophthaloylbis<1,1,1-trimethylhydrazinium> diiodide

Guidance literature:

In acetonitrile; 1.) 70 deg C, 1 h, 2.) 60 deg C, 18 h;

DOI:10.1002/jps.2600750419

upstream raw materials:

N,N-Dimethylhydrazine

benzene-1,3-dicarbonyl dichloride

Downstream raw materials:

2,2'-isophthaloylbis<1,1,1-trimethylhydrazinium> dihydroxide bis(inner salt)

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