2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

Base Information

Chemical Name:2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol
CAS No.:199448-93-6
Molecular Formula:C₂₇H₄₈O₇
Molecular Weight:484.674
Hs Code.:

Synonyms:2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

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Chemical Property of 2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

Chemical Property:

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Technology Process of 2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

There total 13 articles about 2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 199448-92-5
(2-{(S)-2-[2-(2-{(S)-2-[2-(2-Methoxy-ethoxymethoxy)-ethoxy]-4-methyl-pentyloxy}-ethoxy)-ethoxy]-4-methyl-pentyloxy}-ethoxymethyl)-benzene

: 199448-93-6
2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

Guidance literature:: With zinc dibromide; In dichloromethane;
DOI:10.1002/anie.199701221

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 199448-93-6
2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

Guidance literature:: Multi-step reaction with 11 steps

1: 54 percent / aq. NaNO₂, H₂SO₄

2: 75 percent / HCl / toluene

3: 87 percent / TsOH / diethyl ether

4: 94 percent / LiAlH₄ / diethyl ether

5: KOH / tetrahydrofuran

6: TsOH / methanol

7: KOH / tetrahydrofuran

8: TsOH / methanol

9: 90 percent / pyridine

10: 68 percent / KOH / tetrahydrofuran

11: 44 percent / ZnBr₂ / CH₂Cl₂

With pyridine; hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; toluene-4-sulfonic acid; zinc dibromide; sodium nitrite; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1002/anie.199701221

Reference yield:

: 13748-90-8,498-36-2
(S)-2-hydroxyl-3,3-dimethylbutyric acid

: 199448-93-6
2-[(S)-1-(2-{2-[(S)-1-(2-Benzyloxy-ethoxymethyl)-3-methyl-butoxy]-ethoxy}-ethoxymethyl)-3-methyl-butoxy]-ethanol

Guidance literature:: Multi-step reaction with 10 steps

1: 75 percent / HCl / toluene

2: 87 percent / TsOH / diethyl ether

3: 94 percent / LiAlH₄ / diethyl ether

4: KOH / tetrahydrofuran

5: TsOH / methanol

6: KOH / tetrahydrofuran

7: TsOH / methanol

8: 90 percent / pyridine

9: 68 percent / KOH / tetrahydrofuran

10: 44 percent / ZnBr₂ / CH₂Cl₂

With pyridine; hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; toluene-4-sulfonic acid; zinc dibromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1002/anie.199701221