Technology Process of C11H11FN4O2
There total 4 articles about C11H11FN4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
water; N,N-dimethyl-formamide;
at 80 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 8-quinolinol; copper(l) iodide; potassium carbonate / dimethyl sulfoxide / 135 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 °C
3.1: N,N-dimethyl-formamide; water / 2 h / 80 °C
With
copper(l) iodide; 8-quinolinol; potassium carbonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper diacetate; pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 °C
3.1: N,N-dimethyl-formamide; water / 2 h / 80 °C
With
pyridine; copper diacetate; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;