2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

Base Information

Chemical Name:2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate
CAS No.:139415-79-5
Molecular Formula:CF₃O₃S*C₁₉H₂₆NO₃
Molecular Weight:465.491
Hs Code.:

Synonyms:2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

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Chemical Property of 2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

Chemical Property:

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Technology Process of 2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

There total 3 articles about 2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139286-64-9
cyclohexanespiro-3'-(2'-methyl-4'-ethoxycarbonyl-5'-phenyl-4'-isoxazoline)

: 333-27-7
methyl trifluoromethanesulfonate

: 139415-79-5
2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

Guidance literature:: In tetrachloromethane; at 25 ℃; for 2h;
DOI:10.1016/S0040-4020(01)80585-8

Reference yield:

: 58751-78-3
N-cyclohexylidenemethanamine N-oxide

: 139415-79-5
2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tetrahydrofuran / 1 h / 40 °C

2: CCl₄ / 2 h / 25 °C

In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4020(01)80585-8

Reference yield:

: 2216-94-6
phenylpropynoic acid ethyl ester

: 139415-79-5
2,2-dimethyl-3-spirocyclohexyl-4-ethoxycarbonyl-5-phenyl-4-isoxazolinium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tetrahydrofuran / 1 h / 40 °C

2: CCl₄ / 2 h / 25 °C

In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4020(01)80585-8