3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

Base Information

Chemical Name:3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate
CAS No.:1269657-62-6
Molecular Formula:CF₃O₃S*C₁₀H₁₁N₂O₃S
Molecular Weight:388.345
Hs Code.:

Synonyms:3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

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Chemical Property of 3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

There total 3 articles about 3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1198183-95-7
phenyl 1H-imidazole-1-sulfonate

: 333-27-7
methyl trifluoromethanesulfonate

: 1269657-62-6
3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

Guidance literature:: In diethyl ether; at 0 ℃; for 3.5h; Inert atmosphere;
DOI:10.1016/j.tet.2010.11.085

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1269657-62-6
3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / tetrahydrofuran

2: dichloromethane / 0 °C

With caesium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2014.10.065

Reference yield:

: 16475-29-9
phenylchlorosulfate

: 1269657-62-6
3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: diethyl ether / 3.5 h / 0 °C / Inert atmosphere

In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.tet.2010.11.085