3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Base Information

Chemical Name:3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone
CAS No.:1279096-45-5
Molecular Formula:C₂₂H₁₉ClN₂O₆S
Molecular Weight:474.922
Hs Code.:

Synonyms:3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Suppliers and Price of 3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

There total 5 articles about 3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1279096-41-1
3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

: 1279096-45-5
3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Guidance literature:: With ammonia; In methanol; at 0 ℃; for 0.5h;
DOI:10.1080/15257770.2010.551646

Reference yield:

: 99-91-2
para-chloroacetophenone

: 1279096-45-5
3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium acetate / 0.08 h / Microwave irradiation

2: ammonium sulfate / Inert atmosphere; Heating

3: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 5 - 20 °C

4: ammonia / methanol / 0.5 h / 0 °C

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; ammonium acetate; ammonia; In methanol; acetonitrile;
DOI:10.1080/15257770.2010.551646

Reference yield:

: 77607-77-3
3-cyano-6-(4'-chlorophenyl)-4-(thiophen-2'-yl)-2(1H)-pyridone

: 1279096-45-5
3-cyano-6-(4'-chlorophenyl)-1-(β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium sulfate / Inert atmosphere; Heating

2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 5 - 20 °C

3: ammonia / methanol / 0.5 h / 0 °C

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; ammonia; In methanol; acetonitrile;
DOI:10.1080/15257770.2010.551646