3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Base Information

Chemical Name:3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone
CAS No.:1279096-41-1
Molecular Formula:C₃₀H₂₇ClN₂O₁₀S
Molecular Weight:643.071
Hs Code.:

Synonyms:3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

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Chemical Property of 3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

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Technology Process of 3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

There total 5 articles about 3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 77607-77-3
3-cyano-6-(4'-chlorophenyl)-4-(thiophen-2'-yl)-2(1H)-pyridone

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1279096-41-1
3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Guidance literature:: With potassium hydroxide; In water; acetone; at 20 ℃;
DOI:10.1080/15257770.2010.551646

Reference yield:

: C₁₉H₁₇ClN₂OSSi

: 604-68-2
α-D-glucopyranose peracetylate

: 1279096-41-1
3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 5 - 20 ℃;
DOI:10.1080/15257770.2010.551646

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 1279096-41-1
3-cyano-6-(p-chlorophenyl)-1-(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)-4-(thiophen-2'-yl)-2-pyridone

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / 0.08 h / Microwave irradiation

2: ammonium sulfate / Inert atmosphere; Heating

3: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 5 - 20 °C

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; ammonium acetate; In acetonitrile;
DOI:10.1080/15257770.2010.551646