1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene

Base Information

• Chemical Name: 1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene
• CAS No.: 213313-12-3
• Molecular Formula: C₂₀H₂₄O₆
• Molecular Weight: 360.407

Synonyms:1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene

Chemical Property of 1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene

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Technology Process of 1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene

There total 1 articles about 1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

O-methoxymethylisovanillin (5779-98-6) + [(3,4,5-trimethoxyphenyl)methyl]phosphoric acid diethyl ester (134029-74-6) → 1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene (213313-12-3)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran;

DOI:10.1016/S0960-894X(98)00344-8

Reference yield: 89.0%

1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene (213313-12-3) → (1S,2S)-1-(4-Methoxy-3-methoxymethoxy-phenyl)-2-(3,4,5-trimethoxy-phenyl)-ethane-1,2-diol (213313-13-4)

Guidance literature:

With AD-mix-α; methanesulfonamide; In dichloromethane; water; tert-butyl alcohol;

DOI:10.1016/S0960-894X(98)00344-8

Reference yield: 76.0%

1,2,3-Trimethoxy-5-[(E)-2-(4-methoxy-3-methoxymethoxy-phenyl)-vinyl]-benzene (213313-12-3) → (1R,2R)-1-(4-Methoxy-3-methoxymethoxy-phenyl)-2-(3,4,5-trimethoxy-phenyl)-ethane-1,2-diol (213313-09-8)

Guidance literature:

With methanesulfonamide; AD-mix-β; In dichloromethane; water; tert-butyl alcohol;

DOI:10.1016/S0960-894X(98)00344-8

upstream raw materials:

O-methoxymethylisovanillin

[(3,4,5-trimethoxyphenyl)methyl]phosphoric acid diethyl ester

Downstream raw materials:

(1S,2S)-1-(4-Methoxy-3-methoxymethoxy-phenyl)-2-(3,4,5-trimethoxy-phenyl)-ethane-1,2-diol

(1R,2R)-1-(4-Methoxy-3-methoxymethoxy-phenyl)-2-(3,4,5-trimethoxy-phenyl)-ethane-1,2-diol

(4S,5S)-4-(4-Methoxy-3-methoxymethoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-[1,3]dioxolane

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