(4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

Base Information

Chemical Name:(4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate
CAS No.:1276111-31-9
Molecular Formula:CF₃O₃S*C₂₂H₂₀IO
Molecular Weight:576.375
Hs Code.:

Synonyms:(4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

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Chemical Property of (4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

Chemical Property:

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Technology Process of (4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

There total 2 articles about (4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 25116-37-4
3-iodobenzophenone

: 108-67-8
1,3,5-trimethyl-benzene

: 1276111-31-9
(4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

Guidance literature:: 3-iodobenzophenone; 1,3,5-trimethyl-benzene; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

trifluorormethanesulfonic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/ja2008906

Reference yield:

: 2835-78-1
3-amino benzophenone

: 1276111-31-9
(4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / acetonitrile

1.2: 2.5 h / 0 - 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane

2.2: 3 h / 0 - 20 °C

With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1021/ja2008906

Reference yield:

: 1276111-31-9
(4-(phenylcarbonyl)phenyl)(mesityl)iodonium trifluoromethylsulfonate

: 22161-81-5,22161-86-0
S-ketoprofen

Guidance literature:: Multi-step reaction with 2 steps

1: (2R,5R)-2-tert-butyl-3-methyl-5-phenyl-4-imidazolidinone trichloroacetic acid salt; sodium hydrogencarbonate; copper(I) bromide / diethyl ether; toluene / 3 h / 0 °C / Inert atmosphere

2: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / diethyl ether; water; toluene; acetonitrile / 3 h / 20 °C

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; (2R,5R)-2-tert-butyl-3-methyl-5-phenyl-4-imidazolidinone trichloroacetic acid salt; sodium hydrogencarbonate; copper(I) bromide; In diethyl ether; water; toluene; acetonitrile;
DOI:10.1021/ja2008906