C₂₈H₂₃ClN₂O₃

Base Information

Chemical Name:C₂₈H₂₃ClN₂O₃
CAS No.:1422166-88-8
Molecular Formula:C₂₈H₂₃ClN₂O₃
Molecular Weight:470.955
Hs Code.:

C<sub>28</sub>H<sub>23</sub>ClN<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₈H₂₃ClN₂O₃

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Chemical Property of C₂₈H₂₃ClN₂O₃

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Technology Process of C₂₈H₂₃ClN₂O₃

There total 7 articles about C₂₈H₂₃ClN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 28022-43-7
p-chlorobenzhydrylamine

: 1422169-53-6
2-(2-(3,5-dimethylisoxazol-4-yl)benzofuran-5-yl)acetic acid

: 1422166-88-8
C₂₈H₂₃ClN₂O₃

Guidance literature:: 2-(2-(3,5-dimethylisoxazol-4-yl)benzofuran-5-yl)acetic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 2h;

p-chlorobenzhydrylamine; With benzotriazol-1-ol; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1422166-88-8
C₂₈H₂₃ClN₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid / 0 - 80 °C

2.1: triethylamine; magnesium chloride / acetonitrile / Inert atmosphere; Reflux

3.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C

3.2: 3 h / 0 °C

4.1: potassium phosphate; copper(l) iodide / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

5.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 4 h / 80 °C / Inert atmosphere

6.1: sodium hydroxide / water; methanol / 2 h / 20 °C

6.2: pH 4

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 2 h / 20 °C

7.2: 24 h / 20 °C

With potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; magnesium chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 1422166-88-8
C₂₈H₂₃ClN₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine; magnesium chloride / acetonitrile / Inert atmosphere; Reflux

2.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C

2.2: 3 h / 0 °C

3.1: potassium phosphate; copper(l) iodide / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 4 h / 80 °C / Inert atmosphere

5.1: sodium hydroxide / water; methanol / 2 h / 20 °C

5.2: pH 4

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 2 h / 20 °C

6.2: 24 h / 20 °C

With potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; magnesium chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; acetonitrile;