(S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate

Base Information

Chemical Name:(S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate
CAS No.:1334324-79-6
Molecular Formula:C₂₂H₂₄N₂O₄
Molecular Weight:380.444
Hs Code.:

Synonyms:(S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate

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Technology Process of (S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate

There total 2 articles about (S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 115329-03-8
((S)-1-Allylcarbamoyl-2-phenyl-ethyl)-carbamic acid benzyl ester

: 1334324-79-6
(S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 45 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol202276h

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 1334324-79-6
(S,E)-benzyl (1-oxo-1-((4-oxopent-2-en-1-yl)amino)-3-phenylpropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 0 °C / Inert atmosphere

2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 6 h / 45 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/ol202276h