1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

Base Information

Chemical Name:1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride
CAS No.:87761-60-2
Molecular Formula:C₂₂H₃₁N₅O*ClH
Molecular Weight:417.982
Hs Code.:

Synonyms:1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

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Chemical Property of 1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

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Technology Process of 1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

There total 5 articles about 1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 774498-96-3
3-<(1-adamantyl)methoxy>aniline

: 127099-85-8,780722-26-1,461-58-5
N-Cyanoguanidine

: 67-64-1
acetone

: 87761-60-2
1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

Guidance literature:: With hydrogenchloride; for 24h; Heating;
DOI:10.1021/jm00390a017

Reference yield:

: 770-71-8
1-adamantanemethanol

: 87761-60-2
1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 12 g / pyridine

2: K₂CO₃ / dimethylformamide / 40 h / Heating

3: 100 percent / H₂ / 5percent Pd/C / ethanol

4: 40 percent / conc. HCl / 24 h / Heating

With pyridine; hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00390a017

Reference yield:

: 828-51-3
1-Adamantanecarboxylic acid

: 87761-60-2
1-[3-(Adamantan-1-ylmethoxy)-phenyl]-6,6-dimethyl-1,6-dihydro-[1,3,5]triazine-2,4-diamine; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 8.0 g / LiAlH₄ / tetrahydrofuran / 16 h / 0 °C

2: 12 g / pyridine

3: K₂CO₃ / dimethylformamide / 40 h / Heating

4: 100 percent / H₂ / 5percent Pd/C / ethanol

5: 40 percent / conc. HCl / 24 h / Heating

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00390a017