di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

Base Information

Chemical Name:di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12
CAS No.:78631-01-3
Molecular Formula:C₃₄H₅₀N₄O₁₁S₂
Molecular Weight:754.923
Hs Code.:

Synonyms:di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

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Technology Process of di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

There total 12 articles about di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 78600-10-9
N-p-toluenesulfonyl-1-trioxa-4,10,16-triaza-1,7,13-cyclooctadecane

: 78630-99-6
dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

: 78631-01-3
di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

Guidance literature:: With triethylamine; In toluene; for 6h;
DOI:10.1002/hlca.19810640410

Reference yield:

: C₁₃H₁₉Cl₂NO₅S

: 78631-01-3
di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide

2: (i) Ba(OH)2, (ii) aq. HCl

3: (COCl)2

With oxalyl dichloride; In N,N-dimethyl-formamide;
DOI:10.1021/ja00850a051

Reference yield:

: C₁₅H₁₉N₃O₅S

: 78631-01-3
di-p-toluenesulfonyl-7,9-pentaoxa-4,10,16,22,27-tetraaza-1,7,13,19-bicyclo<11.11.5>nonacosanedione-2,12

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Ba(OH)2, (ii) aq. HCl

2: (COCl)2

With oxalyl dichloride;
DOI:10.1021/ja00850a051