N-phenylspiro<4,5-diazatricyclo<4.3.0.0^3,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide

Base Information

• Chemical Name: N-phenylspiro<4,5-diazatricyclo<4.3.0.0^3,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide
• CAS No.: 98816-44-5
• Molecular Formula: C₁₇H₁₇N₃O₄
• Molecular Weight: 327.34

Synonyms:N-phenylspiro<4,5-diazatricyclo<4.3.0.0^3,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide

Chemical Property of N-phenylspiro<4,5-diazatricyclo<4.3.0.0^3,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide

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Technology Process of N-phenylspiro<4,5-diazatricyclo<4.3.0.0^3,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide

There total 3 articles about N-phenylspiro<4,5-diazatricyclo<4.3.0.0^3,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

8-oxo-N-phenyl-4,5-diazatricyclo<4.3.0.03,7>nonane-4,5-dicarboxamide (96227-96-2) + ethylene glycol (107-21-1) → N-phenylspiro<4,5-diazatricyclo<4.3.0.03,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide (98816-44-5)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 5h; Heating;

Reference yield:

norborn-5-en-2-one (694-98-4) → N-phenylspiro<4,5-diazatricyclo<4.3.0.03,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide (98816-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 9 percent / 1,1,2,2-tetrachloroethane / 48 h / 75 - 80 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 5 h / Heating

With toluene-4-sulfonic acid; 1,1,2,2-tetrachloroethane; In toluene;

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → N-phenylspiro<4,5-diazatricyclo<4.3.0.03,7>nonane-8,2'-<1,3>dioxolane>-4,5-dicarboximide (98816-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 9 percent / 1,1,2,2-tetrachloroethane / 48 h / 75 - 80 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 5 h / Heating

With toluene-4-sulfonic acid; 1,1,2,2-tetrachloroethane; In toluene;

upstream raw materials:

8-oxo-N-phenyl-4,5-diazatricyclo<4.3.0.0^3,7>nonane-4,5-dicarboxamide

ethylene glycol

4-Phenyl-1,2,4-triazolidine-3,5-dione

norborn-5-en-2-one

Downstream raw materials:

spiro<1,3-dioxolane-2,3'-tricyclo<3.2.0.0^2,7>heptane>

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