ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

Base Information

Chemical Name:ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside
CAS No.:1443034-31-8
Molecular Formula:C₅₀H₄₉NO₁₁S
Molecular Weight:872.005
Hs Code.:

Synonyms:ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

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Chemical Property of ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

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Technology Process of ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

There total 8 articles about ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1443034-28-3
ethyl 2,3,4-tri-O-benzoyl-1-thio-β-D-mannopyranoside

: 88574-06-5
6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}hexanoic acid

: 1443034-31-8
ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

Guidance literature:: With pyridine; dmap; diisopropyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.201210176

Reference yield:

: 1080665-72-0,686299-00-3
C₈H₁₆O₅S

: 1443034-31-8
ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0 - 80 °C / Inert atmosphere

2: pyridine / 0 - 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / dichloromethane; methanol / 20 °C / Inert atmosphere

4: diisopropyl-carbodiimide; pyridine; dmap / dichloromethane / 0 - 20 °C

With pyridine; dmap; toluene-4-sulfonic acid; diisopropyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1002/anie.201210176

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1443034-31-8
ethyl 2,3,4-tri-O-benzoyl-6-O-(N-fluorenylmethoxycarbonyl-6-aminohexanoyl)-1-thio-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; acetone / 12 h / 20 °C / Inert atmosphere

2: diisopropyl-carbodiimide; pyridine; dmap / dichloromethane / 0 - 20 °C

With pyridine; dmap; sodium hydrogencarbonate; diisopropyl-carbodiimide; In dichloromethane; water; acetone;
DOI:10.1002/anie.201210176